Lead halide perovskites have attracted considerable interest in the recent decade owing to high performance and possible utility in photovoltaics, light emitting diodes and optoelectronics. In this project, inverse temperature crystallization (ITC) was employed to synthesize large, high-quality single crystals of the metal halide perovskites. Bench scale synthesis pathways were adapted to be compatible with liquid handlers, providing a route for high-throughput robotic exploration of this chemical space. In addition, the large set of crystallization outcome data generated during the robotic runs as a function of reagents and reaction conditions was used to probe the synthesis-structure relationship in lead halide perovskites, opening up the possibility for targeted syntheses in the near future.<br/>

Robot-ready, high throughput synthesis of lead halide perovskites

2019 Spring National Meeting

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